Preparation and characterization of series polyimides

Ren, Feifei and Wang, Yongwei and Li, Huang and Wang, Xiaojie and Wang, Jing (2009) Preparation and characterization of series polyimides. China Synthetic Resin and Plastics, 26 (2). pp. 19-22. ISSN 1002-1396

Abstract

A series of poly (amide acid)s (PAA) and polyimides (PI) films were synthesized from the dianhydride monomer of 4,4'-oxydiphthalic dianhydride (ODPA) and the diamine monomer of 1,4-phenylenediamine (PDA) and 4,4'-oxydianiline (ODA) respectively with low temperature condensation process. The structures and mechanical properties of PAA and PI were analyzed by means of Fourier transform infrared spectroscopy (FTIR) and universal material tester. The mechanical properties of the ODPA-PDA and ODPA-ODA films were compared. The results indicate that the imidization of PAA is almost fully completed; the elemental composition and spatial configuration of the polymer chain segment have remarkable influence on the mechanical properties of PAA and PI films. The tensile strength of the PI(ODPA-PDA) thin film reaches 450 MPa.


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Item Type: Article (Commonwealth Reporting Category C)
Refereed: Yes
Item Status: Live Archive
Faculty / Department / School: Historic - Faculty of Engineering and Surveying - Department of Mechanical and Mechatronic Engineering
Date Deposited: 14 Oct 2014 05:14
Last Modified: 07 Nov 2014 04:53
Uncontrolled Keywords: film; imidization; poly (amide acid); polyimide
Fields of Research : 03 Chemical Sciences > 0303 Macromolecular and Materials Chemistry > 030305 Polymerisation Mechanisms
01 Mathematical Sciences > 0101 Pure Mathematics > 010106 Lie Groups, Harmonic and Fourier Analysis
09 Engineering > 0913 Mechanical Engineering > 091307 Numerical Modelling and Mechanical Characterisation
Socio-Economic Objective: E Expanding Knowledge > 97 Expanding Knowledge > 970109 Expanding Knowledge in Engineering
URI: http://eprints.usq.edu.au/id/eprint/25700

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